farmatsevtik kimyo ibodov 1 qism

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o'zbekiston respublikasi sog‘liqni saqlash vazirligi toshkent farmatsevtika instituti a.yu. ibodov, a.n. yunusxo‘jayev, q.a. ubaydullayev f a r m a t s e v t i k k i m y o i qism o ‘zbekiston respublikasi oliy va o ‘rta maxsus ta 'lim vazirligi farmatsevtika oliy ta ’lim muassasasi talabalari uchun darslik sifatida tavsiya etgan toshkent «voris-nashriyot» 2011 o'zbekiston respublikasi davlat mustaqilligining 20 yilligiga bag ishlanadi 35.66 1-13 ibodov, a. yu. farmatsevtik kimyo : [2 qismli] / a. yu. ibodov, a. n. yunusxo‘ja-yev, q. a. ubaydullayev; 0 ‘zr sog‘liqni saqlash vazirligi, toshkent far-matsevtika in-ti. - t .: voris, 2011. - q. i. - 584 b. i. yunusxo‘jayev, a. n. ii. ubaydullayev, q. a. bbk 35.66 udk 681.7 taqrizchilar: o.a. shabilolov - toshkent farmatsevtika instituti ilmiy ishlar va axborot texnologiyalari bo'yicha prorektori, professor, a.f. do'smatov - dori vositalari va tibbiy texnika sifatini nazorat qilish bosh boshqarmasi dori vositalari sifatini nazorat qilish …

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.........................................................................................11 i bo‘lim. umumiy farmatsevtik kimyo 1-bob. farmatsevtik kimyo fanining nazariy asoslari.................................. 13 1.1. farmatsevtik kimyo fani, uning mohiyati va obyektlari.............................13 1.2. farmatsevtik kimyo fanining qisqacha tarixi...............................................16 1.3. dori moddalarining tasnifi (klassifikatsiyasi).............................................. 23 dori moddalarini olish manbalari........................................................................ 27 yangi dori moddalarini yaratish borasida ba’zi ilmiy izlanishlar..................... 29 2-bob. o'zbekiston respublikasida dori vositalari sifatini ta ’minlash m asalalari.......................................................................................... 32 2.1. sifat nazorati me’yoriy texnik hujjatlari ishlab chiqish tartibi va ulaming mazmuni..............................................................................................32 dori vositalari davlat standartlari........................................................................ 34 dori moddasi (substansiya) uchun me’yoriy hujjatning tuzilishi................... . 36 2.2. dori moddalari sifatini nazorat qilish davlat tizim i.....................................45 2.3. farmatsevtika ishlab chiqarish korxonalarida dori vositalari sifatini nazorat qilishni uyushtirish...................................................................... 49 2.4. nazorat-tahlil laboratoriyalarida dori vositalari sifat nazoratini uyushtirish............................................................................................................... 53 3-bob. dori moddalari chinligini aniqlashning umumiy usu ilari...............56 3.1. fizikaviy usullar bo'yicha dori moddalari chinligini aniqlash...................57 3.2. kimyoviy usullar bo'yicha dori moddalari chinligini aniqlash................. 61 anionlami a

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niqlash.................................................................................................66 4-bob. dori moddalari tarkibiga yot m oddalam ing qo‘shilib qolish manbalari va sabab la ri........................................................................................73 5-bob. dori moddalari m iqdorini tahlil qilish u su ila ri.................................77 5.1. gravimetrik (tortma) u su l.............................................................................. 79 5.2. titrimetrik (hajmiy) usu l................................................................................80 a. cho‘ktirishga asoslangan usullar.....................................................................81 b. kislota-asos titrlash (neytrallash) usuli...........................................................88 d. suvsiz muhitda kislota-asos titrlash usuli.......................................................92 e. oksidlanish-qaytarilish reaksiyasiga asoslangan usullar...............................99 f. kompleksonometrik usu l................................................................................ 110 g. nitritometriya usuli......................................................................................... 116 6-bob. dori moddalari tarkibidagi organik birikkan turli elementlaming miqdorini an iq lash ................................................................ 119 6.1. azotni aniqlash.............................................................................................. 120 6.2. galogenlar. oltingugurt va fosfomi aniqlash............................................ 122 3 7-bob. dori vositalari miqdoriy tahlilining fizikaviy va fizik-kimyoviy u su ila ri.......................................................................................128 7.1. potensiometrik titrlash usuli..... ...................................................................128 7.2. polyarografik usul..................................................................

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$....................... 132 7.3. refraktometrik usu l ...................................................................................... 138 7.4. polyarimetrik usul.........................................................................................149 7.5. elektromagnit nurlanishning yutilishiga asoslangan usullar....................152 7.5.1. tahlilning fotometrik usuilari...................................................................152 ^ 7 .5 .2 . spektrofotometrik usulning moddalar tozaligini aniqlashda qo'llanilishi........................................................................................ 157 \^ f.5 .3 . spektrofotometrik usul yordamida dori vositalarining miqdorini aniqlash................................................................................................159 7.6. iq-spektrofotometrik usul............................................................................172 7.7_fluonmetrik usu l...........................................................................................180 7.8. yadro-magnit rezonansi spektroskopiyasi (yamr, pmr, 13c-yamr) _ 189 7.9. xromatografik usullar..................................................................................197 7.9.1. ion almashinish xromatografiyasi............................................................ 198 7.9.2. taqsimlanish (qog'oz) xromatografiyasi.................................................205 7.9.3. yupqa qatlam xromatografiyasi............................................................... 211 7.9.4. gaz xromatografiyasi.................................................................................218 7.9.5. yuqori samarali suyuqlik xromatografiyasi (yuqori bosim suyuqlik xromatografiyasi)........................................................228 ii bo‘lim. farmatsevtik kimyoning maxsus qismi. noorganik dori moddalari 8-bob. kislorod va uning b irikm alari.............................................................234 kislorod.......................$

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...........................................................................................234 tozalangan suv ..................................................................................................... 237 vodorod peroksid va uning preparatlari.............................................................240 9-bob. o ltingugurt p rep ara tla ri...................................................................... 248 cho'ktirilgan oltingugurt..................................................................................... 249 natriy tiosulfat...................................................................................................... 250 10-bob. galogenlar va ularning ishqoriy metallar bilan bo‘lgan b irikm alari........................................................................................................... 253 _ xlorid kislota.........................................................................................................254 xlorli ohak. oqartirgich ohak 257 natriy va kaliy xlorid............................................................................................259 ̂ natriy va kaliy bromid......................................................................................... 262 4 - y ed_______________ _______________________________ _____________264 natriy va kaliy yodid........................................................................................... 268 11-bob. azot b irikm alari................................................................. ................ 270 azot (i) oksid........................................................................................................270 natriy nitrit............................................................................................................273 12-bob. arsen b irikm alari................................................................................ 274 arsenit angidridi......................................................................

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o'zbekiston respublikasi sog‘liqni saqlash vazirligi toshkent farmatsevtika instituti a.yu. ibodov, a.n. yunusxo‘jayev, q.a. ubaydullayev f a r m a t s e v t i k k i m y o i qism o ‘zbekiston respublikasi oliy va o ‘rta maxsus ta 'lim vazirligi farmatsevtika oliy ta ’lim muassasasi talabalari uchun darslik sifatida tavsiya etgan toshkent «voris-nashriyot» 2011 o'zbekiston respublikasi davlat mustaqilligining 20 yilligiga bag ishlanadi 35.66 1-13 ibodov, a. yu. farmatsevtik kimyo : [2 qismli] / a. yu. ibodov, a. n. yunusxo‘ja-yev, q. a. ubaydullayev; 0 ‘zr sog‘liqni saqlash vazirligi, toshkent far-matsevtika in-ti. - t .: voris, 2011. - q. i. - 584 b. i. yunusxo‘jayev, a. n. ii. ubaydullayev, q. a. bbk 35.66 udk 681.7 taqrizchilar: o.a. shabilolov …

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